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ขุดทดลองการกลั่นแบบเศษส่วนด้วยคอลัมน์ถาดฟองสบู่ด้วย CobraSMARTsense

Fractional distillation with the bubble tray column with CobraSMARTsense

ขุดทดลองการกลั่นแบบเศษส่วนด้วยคอลัมน์ถาดฟองสบู่ด้วย CobraSMARTsense

Article no. : P3031667

Principle

In countercurrent distillation (rectification) using a column, the rising vapour can enter into interactions with the condensate. In this manner, a fractional distillation, i.e. a distillation in several steps for the separation of substances with similar boiling points, can be performed in a single apparatus. If bubble tray columns are used condensate can be removed from the individual bubble trays.

Benefits

  • Simplified implementation: all pre-settings already prepared
  • Didactic gas chromatograph included
  • Glass jacket system easily expandable
  • Simultaneous temperature measurement at four points

Tasks

  1. Investigate the mode of operation of a fractionating tower on a two-stage bubble tray column. Distil a mixture of three n-alcanes first with total reflux and then without any reflux.
  2. Subsequently, examine and compare the initial mixture, the sump product, the head products and the condensates of both trays.

Learning objectives

  1. Bubble tray column
  2. Rectification
  3. Continuous and discontinuous distillation
  4. Vapour pressure
  5. Vaporisation
  6. Condensation
  7. Raoult’s law